Dissolved inorganic carbon, total alkalinity, and other variables collected from profile and discrete observations using Niskin bottle and other instruments from NOAA Ship Ronald H. Brown in the North Atlantic ocean (off the east coast of Florida) during the Ocean Acidification Cruise RB1201 from 2012-02-15 to 2012-03-05 (NCEI Accession 0154381)
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title: Dissolved inorganic carbon, total alkalinity, and other variables collected from profile and discrete observations using Niskin bottle and other instruments from NOAA Ship Ronald H. Brown in the North Atlantic ocean (off the east coast of Florida) during the Ocean Acidification Cruise RB1201 from 2012-02-15 to 2012-03-05 (NCEI Accession 0154381)
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abstract: This dataset contains bottle measurements of dissolved inorganic carbon and total alkalinity off the east coast of Florida. Increasing amounts of atmospheric carbon dioxide from human industrial activities are causing changes in global ocean carbon chemistry. Through the SOOP program we measure air and ocean surface pCO2 and take discrete samples of other carbon parameters. This effort is in support of the coastal monitoring and research objectives of the NOAA Ocean Acidification Program (OAP) and the Climate Program Office.
purpose: To measure key carbon, physical and biogeochemical parameters in coastal waters of the US in relation to Ocean Acidification and monitor changes over time.
credit: Funding Information: NOAA Ocean Acidification Program (Coastal Observations on the East Coast: Ocean Acidification Monitoring Network, OAPFY13.03.AOML.001)
credit: Funding Information: NOAA's Climate Program Office and Ocean Acidification Program (Quantifying sea-air CO2 fluxes using surface water pCO2 measurements from ships of opportunity, Ocean acidification Ship of Opportunity (SOOP))
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beginPosition: 2012-02-15
endPosition: 2012-03-05
supplementalInformation: EXPOCODE: 33RO20120215 CRUISE ID: RB1201 FUNDING AGENCY: NOAA's Climate Program Office, NOAA's Ocean Acidification Program PROJECT TITLE: Quantifying sea-air CO2 fluxes using surface water pCO2 measurements from ships of opportunity, Ocean acidification Ship of Opportunity (SOOP) PRINCIPAL INVESTIGATORS: Rik Wanninkhof {Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA), 4301 Rickenbacker Causeway, Miami, FL, 33149, USA} Leticia Barbero {Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA), 4301 Rickenbacker Causeway, Miami, FL, 33149, USA} Denis Pierrot {Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA), 4301 Rickenbacker Causeway, Miami, FL, 33149, USA} In this accession, NCEI has archived multiple versions of these data. The latest (and best) version of these data has the largest version number.
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Anchor: https://www.ncei.noaa.gov/archive/archive-management-system/OAS/bin/prd/jquery/institution/details/1730 NOAA National Centers for Environmental Information
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description: NCEI Accession 0154381 v1.1 was published.
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DateTime: 2016-07-11T13:19:08Z
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name: NCEI Accession 0154381 v1.1
description: published 2016-07-11T13:19:08Z
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description: NCEI Accession 0154381 was revised and v2.2 was published.
rationale: Updates were received for this dataset. These updates were copied into the data/0-data/ directory of this accession. These updates may provide additional files or replace obsolete files. This version contains the most complete and up-to-date representation of this archival information package. All of the files received prior to this update are available in the preceding version of this accession.
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level: (MD_ScopeCode) dataset
lineage: (LI_Lineage)
processStep: (LE_ProcessStep)
description: Parameter or Variable: Dissolved Inorganic Carbon; Abbreviation: DIC; Unit: micro-mol/kg; Observation type: Profile; In-situ / Manipulation / Response variable: In-situ observation; Measured or calculated: Measured; Sampling instrument: Niskin bottle; Analyzing instrument: Two systems consisting of a coulometer (UIC Inc.) coupled with a Dissolved Inorganic Carbon Extractor (DICE) inlet system. DICE was developed by Esa Peltola and Denis Pierrot of NOAA/AOML and Dana Greeley of NOAA/PMEL to modernize a carbon extractor called SOMMA (Johnson et al. 1985, 1987, 1993, and 1999; Johnson 1992); Detailed sampling and analyzing information: Samples for total dissolved inorganic carbon (DIC) measurements were drawn according to procedures outlined in the Guide to best practices for ocean CO2 measurements (Dickson et al., 2007) from Niskin bottles into cleaned 294-ml glass bottles. Bottles were rinsed and filled from the bottom, leaving 6 ml of headspace; care was taken not to entrain any bubbles. After 0.2 ml of saturated HgCl2 solution was added as a preservative, the sample bottles were sealed with glass stoppers lightly covered with Apiezon-L grease and were stored at room temperature to be sent back to the lab for analysis after the cruise. The analysis was done by coulometry with two analytical systems (AOML3 and AOML4) used simultaneously. In the coulometric analysis of DIC, all carbonate species are converted to CO2 (gas) by addition of excess hydrogen ion (acid) to the seawater sample, and the evolved CO2 gas is swept into the titration cell of the coulometer with pure air or compressed nitrogen, where it reacts quantitatively with a proprietary reagent based on ethanolamine to generate hydrogen ions. In this process, the solution changes from blue to colorless, triggering a current through the cell and causing coulometrical generation of OH minus ions at the anode. The OH ions react with the H+, and the solution turns blue again. A beam of light is shone through the solution, and a photometric detector at the opposite side of the cell senses the change in transmission. Once the percent transmission reaches its original value, the coulometric titration is stopped, and the amount of CO2 that enters the cell is determined by integrating the total charge during the titration. The volume of the pipette used to deliver the sample in each system was determined with aliquots of distilled water at known temperature. The weights with the appropriate densities were used to determine the volume of the pipette. Calculation of the amount of CO2 injected was according to the CO2 handbook (Dickson et al., 2007).The instrument has a salinity sensor, but all DIC values were recalculated to a molar weight (micro-mol/kg) using density obtained from the CTD salinity. The DIC values were corrected for dilution by 0.2 ml of saturated HgCl2 used for sample preservation (Measured DIC*1.00037). A correction was also applied for the offset from the CRM. This additive correction was applied for each cell using the CRM value obtained in the beginning of the cell. Please consult the accompanying Readme file for additional details.; Replicate information: 40 samples each 500-ml, 6 sets of duplicate samples.; Standardization description: The coulometers were calibrated by injecting aliquots of pure CO2 (99.99%) by means of an 8-port valve outfitted with two sample loops with known gas volumes bracketing the amount of CO2 extracted from the water samples for the two AOML systems.; Standardization frequency: The stability of each coulometer cell solution was confirmed three different ways: two sets of gas loops were measured at the beginning; also the Certified Reference Material (CRM), supplied by Dr. A. Dickson of UCSD, were measured at the beginning; and the duplicate samples at the beginning, middle, and end of each cell solution. The coulometer cell solution was replaced after 25 mg of carbon was titrated, typically after 9 to 12 hours of continuous use.; CRM manufacturer: Dr. A. Dickson of UCSD; CRM batch number: Batch 112; Preservation method: saturated HgCl2; Preservative volume: 0.2 ml; Preservative correction: The DIC values were corrected for dilution by 0.2 ml of saturated HgCl2 used for sample preservation. The total water volume of the sample bottles was 288 ml (calibrated by Esa Peltola, AOML). The correction factor used for dilution was 1.00037.; Quality flag convention: WOCE quality control flags are used: 2 = good value, 3 = questionable value, 4 = bad value, 5 = value not reported, 6 = mean of replicate measurements, 9 = sample not drawn.; Method reference: Dickson, A.G., Sabine, C.L. and Christian, J.R. (Eds.) 2007. Guide to best practices for ocean CO2 measurements. PICES Special Publication 3, 191 pp. Johnson, K.M., Kortzinger, A.; Mintrop, L.; Duinker, J.C.; and Wallace, D.W.R. (1999). Coulometric total carbon dioxide analysis for marine studies: Measurement and internal consistency of underway surface TCO2 concentrations. Marine Chemistry 67:123 to 44. Johnson, K.M., Wills, K.D.; Butler, D.B.; Johnson, W.K.; and Wong, C.S. (1993). Coulometric total carbon dioxide analysis for marine studies: Maximizing the performance of an automated gas extraction. Johnson, K.M. (1992). Operator Manual: Single-Operator Multiparameter Metabolic Analyzer (SOMMA) for Total Carbon Dioxide (CT) with Coulometric Detection. Brookhaven National Laboratory, Brookhaven, N.Y. Johnson, K.M.; Williams, P.J.; Brandstrom, L.; and McN. Sieburth, J. (1987). Coulometric total carbon analysis for marine studies: Automation and calibration. Marine Chemistry 21:117 to 33.; Researcher name: Rik Wanninkhof; Researcher institution: Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA).
processStep: (LE_ProcessStep)
description: Parameter or Variable: Total alkalinity; Abbreviation: TAlk; Unit: micro-mol/kg; Observation type: Profile/underway (flow through); In-situ / Manipulation / Response variable: In-situ observation; Measured or calculated: Measured; Sampling instrument: Niskin bottle / flow through system; Analyzing instrument: Semi-automatic titration systems, System 1 consists of a Metrohm 765 Dosimat titrator, a pH meter (Orion 720A, ThermoScientific), a ROSS half cell pH glass electrode (Orion 9101BN, ThermoScientific) and a reference electrode (Orion 900200, ThermoScientific). System 2 consists of a Metrohm 665 Dosimat titrator, a pH meter (Orion 2 star pH Benchtop, ThermoScientific), a ROSS half cell pH glass electrode (Orion 9101BN, ThermoScientific) and a reference electrode (Orion 900200, ThermoScientific).; Type of titration: Full Titration; Cell type (open or closed): Open; Curve fitting method: Least-Square Analysis; Detailed sampling and analyzing information: All of the samples were run using leftover water from the same sample bottles used for DIC and pH. Please refer to DIC for detailed information on sampling and conservation of samples. For each measurement, approximately 200 ml of water sample were titrated with an HCl solution provided by Dr. Andrew Dickson of UCSD (0.25175 moles per kilogram-solution). Please consult the accompanying Readme file for additional details.; Replicate information: 40 samples each 500-ml, 6 sets of duplicate samples.; Standardization description: 2 CRM samples were run daily on each cell, before and after the seawater samples. The Total Alkalinity for the water samples was corrected using the daily averaged ratios between the certified and measured values of the 2 CRMs run on each cell. This TA titration system has a precision of 0.1 %. All the TA values were directly measured with reference to Certified Reference Material. The accuracy after correction is 0.1%. Please check attached pdf for more details.; Standardization frequency: All values were directly measured with reference to Certified Reference Material (Dickson, UCSD). 2 CRM samples were run daily on each cell.; CRM manufacturer: Dr. A. Dickson of UCSD; CRM batch number: CRM batch: 108 and 112; Preservation method: saturated HgCl2; Preservative volume: 0.2 ml; Uncertainty: The precision of this method is better than 0.1% and accuracy is 0.1%.; Quality flag convention: WOCE quality control flags are used: 2 = good value, 3 = questionable value, 4 = bad value, 5 = value not reported, 6 = mean of replicate measurements, 9 = sample not drawn.; Method reference: Millero, F. J., Zhang, J. Z., Lee, K., and Campbell, D. M. (1993). Titration alkalinity of seawater. Marine Chemistry, 44(2), 153-165.; Researcher name: Rik Wanninkhof; Researcher institution: Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA).
processStep: (LE_ProcessStep)
description: Parameter or Variable: Water pressure; Abbreviation: CTDPRS; Unit: decibars; Observation type: Profile; In-situ / Manipulation / Response variable: In-situ observation; Measured or calculated: Measured; Sampling instrument: SBE 911plus CTD; Uncertainty: plus or minus decibar (data has also been vertically binaveraged to 1 decibar bins); Quality flag convention: -999 indicates bad or missing data; Researcher name: Molly Baringer; Researcher institution: Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA).
processStep: (LE_ProcessStep)
description: Parameter or Variable: Water temperature; Abbreviation: CTDTMP; Unit: degrees celsius (ITS-90); Observation type: Profile; In-situ / Manipulation / Response variable: In-situ observation; Measured or calculated: Measured; Sampling instrument: SBE 911plus CTD; Uncertainty: plus or minus 0.001 degrees celsius; Quality flag convention: -999 indicates bad or missing data; Researcher name: Molly Baringer; Researcher institution: Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA).
processStep: (LE_ProcessStep)
description: Parameter or Variable: Salinity; Abbreviation: CTDSAL; Unit: practical salinity scale of 1978; Observation type: Profile; In-situ / Manipulation / Response variable: In-situ observation; Measured or calculated: Seasave 7, calculated from temperature and conductivity; Sampling instrument: SBE 911plus CTD; Detailed sampling and analyzing information: CTD Salinity values were validated using water samples collected during profiles. Corrections were applied when needed.; Uncertainty: plus or minus 0.01 PSS-78; Quality flag convention: -999 indicates bad or missing data; Researcher name: Molly Baringer; Researcher institution: Atlantic Oceanographic and Meteorological Laboratory, National Oceanic and Atmospheric Administration (NOAA) .
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maintenanceNote: Metadata are developed, maintained and distributed by NCEI. Updates are performed as needed to maintain currentness.
maintenanceNote: NCEI Accession 0154381 was revised and a new version of the archival package was published. Updates to existing archival packages may provide additional files or replace obsolete files. The latest version contains the most complete and up-to-date representation of this archival information package. All of the files received prior to this update are available in the preceding version of this accession. Please see journal.txt in the /about directory for additional details on changes made.
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organisationName: NOAA National Centers for Environmental Information
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acquisitionInformation: (MI_AcquisitionInformation)
instrument: (MI_Instrument)
identifier: (MD_Identifier)
code: coulometer for DIC measurement
type: coulometer for DIC measurement
description: measures dissolved inorganic carbon (DIC) A known amount of seawater is dispensed into a stripping chamber where it is acidified and purged with an inert gas. The amount of CO2 in the resulting gas stream is determined by absorbing the CO2 in an absorbent. The pH of the solution is monitored by measuring the transmittance .
instrument: (MI_Instrument)
identifier: (MD_Identifier)
code: titrator
type: titrator
description: titrator
platform: (MI_Platform)
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code: NOAA Ship Ronald H. Brown
description: Updated information from ICES for UNITED STATES platform Ronald H. Brown Flag : UNITED STATES - US (ISO Country Code) Call Sign : WTEC Title : NOAA Ship Platform Class : Research vessel IMO : 9105786 Pennant : R 104 Commissioned Date : 1997-07-19 Current Length : 83.5 Built : 1997 Information Source : http://www.moc.noaa.gov/rb/index.html (URL) Lloyds URL : http://www.seasearcher.com/lmiu/vessels/overview.htm?vesselID=277516 *General Comments:* Name RESEARCHER II planned during build was never used.
instrument: (missing)